3-羟基吡啶 产品编号: YZH137 中文名称: 3-羟基吡啶[1]
3-Hydroxypyridine 中文别名:3-吡啶酚; 3-吡啶酮; 氮苯酮[1] 英文名称: 3-Hydroxypyridine 英文别名: 3-Pyridinol;3-Pyridone 纯度: ≥98% CAS号: 109-00-2[1] 分子式: C5H5NO[1] 分子量: 95.1[1] 分子结构图:右图 由吡啶经磺化、碱熔、中和而得。将发烟硫酸加入干燥的反应锅内,搅拌下滴加吡啶,再加入硫酸汞。加热至230-240℃,保温13-14h。冷至20-25℃,加入乙醇中,继续冷至5℃以下,析出结晶。过滤,得吡啶-3-磺酸。熔点345℃,收率62%。将氢氧化钠及吡啶-3-磺酸加入反应锅内,在160℃熔融,升温至220-230℃保温4h。冷至100℃,加水溶解,用30%的盐酸调节pH至4,减压浓缩,过滤 除去氯化钠。滤液用饱和碳酸钠调节pH至8-9,冷却过滤,烘干,得3-羟基吡啶粗品,收率64%。用甲苯进行重结晶而得精品,熔点126-128℃,含量98%,精制收率80%。
Currently, our company primarily produces halogen compounds, pyridine derivatives, and other organic intermediates. Most of our products are exported to the European, American, Japanese, and Indian markets, which has made us a qualified supplier for many well-known pharmaceutical companies.
The company pays close attention to the new demands of domestic and international markets with its keen vision. From the beginning, it has adhered to the business principle of "the lowest price, the best products," providing customers with excellent services.
We warmly welcome friends from all over the world to visit our company for inspection and discussion. We sincerely hope to further expand trade relations on the basis of mutual benefit, in order to achieve common prosperity and development.